Antinociceptive; Alpha-2 Adrenergic Agonist Xylazine 7361-61-7 Analgesic, Anesthetic

Antinociceptive; Alpha-2 Adrenergic Agonist Xylazine 7361-61-7 Analgesic, Anesthetic

Brand:
Lingding
Place of origin:
China
Model Number:
ldswkj1-3-15?
Weight:
50g
Minimum Orders:
50g
Available:
10
Price:
$12
 
 
Ship To (shipping cost):
Australia ($12), Brazil ($12)
Packing:
carbon capsule
Delivery Time:
3
Payments:
Payments
Guarantee:
Get the item you ordered or get your money back.

Seller Details

Rating:

positive ratings
Location:
China
Joined:
24 September 2021
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Product Description

2,6-Dimethylphenyl isothiocyanate, 31.0 g (0.2 mole), prepared from 2,6- dimethylaniline with thiophosgen, were added dropwise during 15 min to a well-stirred suspension of 15.0 g (0.2 mole) of 3-aminopropanol-1 in 100 ml of ether. The ether started to boil. Stirring under reflux was continued for 30 min, and the ether was then distilled off. The residue was treated with 100 ml of concentrated hydrochlor acid and boiled under reflux for 30 min. After cooling, it was diluted with water, filtered free from impurities, and the base was precipitated by the addition of concentrated sodium hydroxid solution. When recrystallized from benzene-ligroin, the resulting compound 2-(2,6- dimethyl-phenylamino)-4H-5,6-dihydro-1,3-thiazine, melting point 140-142°C (yield 90% of the theoretical).

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